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lead tetraacetate



Hi folks,

After nearly a decade away from lead chemistry I am returning to my 
roots and doing some lead(IV) chemistry.  About <-that-> long ago we 
used to swear by Merck LTA and swear at the inferior product from 
Aldrich. About 2 years ago somoeone in our lab ordered a bottle of Merck 
LTA (CAS 546-67-8, old Merck cat number is:  8.07418), the stuff 
moistened with ~15% glacial acetic acid. It was/is good stuff but we are 
nearly out. I contacted Merck and they no longer supply it.  (The 
salesperson actually offered me lead (II) acetate as a "replacement" 
(Where do they find these people?)

Anyway, can anyone recommend a replacement?  Something you know to be 
reproducibly good as per iodometric titration etc...?  Any 
recommendations for brands to avoid as well would be appreciated. 

cheers,
Martin

_____________________________________________________
  Dr. Martin Stoermer

  INSTITUTE FOR MOLECULAR BIOSCIENCE
  incorporating
  The Centre for Molecular and Cellular Biology
  The Centre for Drug Design and Development
  ARC Special Research Centre for Functional and Applied Genomics

  University of Queensland 4072 AUSTRALIA
  Phone: +61-7-3346 2988   Fax: +61-7-3346 2101
  Email:[EMAIL PROTECTED]
  http://www.imb.uq.edu.au
_____________________________________________________
-- 
Paul J. Franklin(moderator - sci.chem.organic.synthesis) 
http://organicworldwide.net/sci.chem.organic.synthesis
Georgia State University <[EMAIL PROTECTED]>
Atlanta, GA



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